Commands and Tips for Third-Party Devices
Agilent 1100/1200 HPLC System: DAD and MWD Detectors
In addition to (or different from) the standard detector commands (see Commands for Controlling Dionex Devices Dionex Detectors) and the general commands for the 1100/1200 HPLC system (see Agilent 1100/1200 HPLC System: General), the following commands and properties are available (please note that the display Filter level determines which commands and properties are displayed):
UV_VIS Channel Commands
Property |
Description |
AnalogAttenuation |
Attenuation of the analog output (signal value that corresponds to the maximum output voltage). Values: -10 (º 2^-10 AU) - 1(º 2 AU); default: 0 Note: logarithmic scale |
AnalogOffset |
Zero offset of the analog output in % of the full output range. Values: 1 - 99%; default: 5 |
AnalogRange |
Voltage range of the analog output (may be set to 0.1 or 1.0V only). |
Signal bandwidth. Values: 2 - 400 nm |
|
Maximum signal and spectra data rate if Step = Auto. Values: 0.1 s - 5.1 s; default: 0.1x |
|
Reference bandwidth (set to 0 if RefWavelength = 0). Values: 0; 2 - 400 nm |
|
Reference wavelength (0 means: not used). Values: 0; 190 - 950 nm |
|
Signal and spectra data rate (If you set the step, you must set the PeakWidth too, see below). Values: 0.05 - 3.2 s; default: 0.4 s |
|
Signal wavelength. Values: 190 - 950 nm |
The relation between the expected PeakWidth and the corresponding Step is as follows:
Expected peak width [min] |
0.00 |
0.01 |
0.02 |
0.05 |
0.10 |
0.20 |
0.40 |
0.85 |
Corresponding step [s] |
0.05 |
0.05 |
0.10 |
0.20 |
0.40 |
0.80 |
1.60 |
3.20 |
3DFIELD Channel Commands (DAD only)
Property |
Description |
Bandwidth of the 3D wavelength. Values: 0.01 - 100 nm; default: 2 nm |
|
MaxWavelength |
Maximum 3D wavelength. Values: 190 - 950 nm; default: 400 |
MinWavelength |
Minimum 3D wavelength. Values: 190 - 950 nm; default: 190 |
Other Special Detector Commands
Property |
Description |
AutoActivateUV_Lamp |
If set to On, the deuterium lamp is automatically turned on upon power-up. Values: On, Off (default) |
AutoactivateVisible_ |
If set to On, the Tungsten lamp is automatically turned on right after power-up of the detector. Values: On, Off (default) |
Autozero
|
Performs Autozero. The command is performed immediately, when issued manually, or at a Program time <0.000 min. With a program time of 0.000, the command is performed before the injection program; with a program >0.000, the command is performed at this program time. |
DemoFileName |
File name of the demo file. (May contain %d that will be replaced by the sample number) |
PeakWidth
|
Expected minimum peak width in [min] (If you set the PeakWidth, you must also set the Step: see above). Values (Agilent 1100/1200 DAD): 0.00, 0.01, 0.02, 0.05, 0.10, 0.20, 0.20, 0.40, 0.85. Values (Agilent 1200 DAD SL): 0.00, 0.0025, 0.0050, 0.01, 0.02, 0.05, 0.10, 0.20, 0.20, 0.40, 0.85. |
SlitWidth |
Width of the micro slit (also MWD). A small slit allows using the fine structures of the UV spectrum. A wide slit provides higher sensitivity. Values: 1 - 16 nm; default: 4 nm |
UV_Lamp |
Reports the state of the deuterium lamp. Values: On, Off (default) |
UV_LampRequired |
If set to On: The detector is not ready for operation if the deuterium lamp is off. Values: On, Off (default) |
Visible_Lamp |
Tungsten lamp state. Values: On, Off (default) |
Visible_LampRequired |
If set to On: The detector is not ready for operation if the Tungsten lamp is off. Values: On, Off (default) |
Counters
The values are read from the module on connect.
Property |
Description |
FilterMovements |
Counter for the movements of the holmium oxide filter. Set the UpperLimit to 0 to disable the associated limit test. |
SlitMovements |
Slit movement counter. Set the UpperLimit to 0 to disable the associated limit test. |
UvLampIgnitions |
UV lamp ignition counter. Set the UpperLimit to 0 to disable the associated limit test. |
UvLampAge |
Total burn time of the UV lamp [h] Set the UpperLimit to 0 to disable the associated limit test. |
UvLampOntime |
Burn time of the UV lamp since the last time it was turned on. Set the UpperLimit to 0 to disable the associated limit test. |
VisLampIgnitions |
VIS lamp ignition counter. Set the UpperLimit to 0 to disable the associated limit test. |
VisLampAge |
Total burn time of the VIS lamp [h]] Set the UpperLimit to 0 to disable the associated limit test. |
VisLampOntime |
Burn time of the VIS lamp since the last time it was turned on. Set the UpperLimit to 0 to disable the associated limit test. |
UV Calibration Commands
Property |
Description |
Adjust_Calibration |
Adjusts the wavelength calibration using the results of a previous wavelength calibration (absolute deviation). |
D2_Alpha_Deviation_ |
Current deviation of D2 alpha or D2 beta line from factory calibration. Valid only after the Test_Calibration command has been completed. |
D2_Alpha_Deviation_ |
Current calibration for the D2 alpha or D2 beta line. Values: -2.000 - 2.000 nm (read from module on connect) |
D2_Alpha_Deviation_ |
Current deviation of the D2 alpha or D2 beta line, considering current wavelength calibration. Values: -2.000 - 2.000 nm Valid only after the Test_Calibration command has been completed. |
Test_Calibration |
Performs a wavelength calibration test as described in the Agilent VWD Detector Reference Manual. You need to remove the flow cell before executing this command. In addition, the UV lamp must be on. |
Diagnostic Commands and Properties
Command |
Description |
CellTest |
Performs a cell test. |
CellTestEvaluation |
Evaluates the cell test by averaging the spectra of all test data. |
CellTestInfo |
Indicates whether the cell test in the next step is performed with or without cell. |
DarkCurrentTest |
Performs a dark current test. |
DarkCurrentTestEvaluation |
Evaluates the dark current test by averaging the minimum and maximum values of all selected spectra ranges. |
FilterTest |
Performs a holmium filter test. |
FilterTestEvaluation |
Evaluates the holmium filter test. |
IntensityTest |
Performs an intensity test. |
IntensityTestEvaluation |
Evaluates the intensity test by calculating the minimum and maximum values of the 1024 diodes for all test data. |
For more information about the diagnostic functions for the DAD detector, refer to:
Agilent 1100 HPLC System Diagnostics: Dark Current Test
Agilent 1100 HPLC System Diagnostics: Cell Test
Agilent 1100 HPLC System Diagnostics: Filter Test
Agilent 1100 HPLC System Diagnostics: Intensity Test
Note:
If the detector is equipped with a "B" firmware version (for example, B.06.14), it is not possible to run diagnostics tests in Chromeleon. Use the Agilent Lab Advisor instead.
The Administrator Help section provides general information and installation instructions for the 1100 and 1200 HPLC systems; refer to Hardware Installation: