Thermo Scientific Detectors
Thermo Scientific Vanquish Diode Array Detector

The commands listed below are available for the Vanquish DAD detector. Please note that the display Filter level and detector type determine which commands and properties are displayed.

3DFIELD channel

Command/Property

Description

AcqOn/Off

Use this command to start/stop data acquisition.

BunchWidth

Use this property to specify the range that is averaged when collecting 3D data (similar to the Bandwidth of a UV channel). A higher BunchWidth reduces the required data storage and improves the signal-noise-ratio, but reduces the Optical Resolution.

 Note: 

Only integer values are accepted. If you enter a decimal value, Chromeleon automatically rounds to an integer value.

MaxWavelength

Use this property to set the maximum wavelength for recording spectra. Narrows the range in which the 3D field is recorded (also see MinWavelength).

MinWavelength

Use this property to set the minimum wavelength for recording spectra. Narrows the range in which the 3D field is recorded (also see MaxWavelength).

RefBandwidth

Use this property to average several photodiode signals of the reference signal. It is not necessary to select a reference bandwidth unless  a reference wavelength is set.

RefWavelength

Use this property to correct the 3D field absorption values. The selected reference wavelength should be in an area of the spectrum where little absorption occurs.

Retention

Indicates the retention time of the signal.

UV channel

 

Command/Property

Description

AcqOn/Off

Use this command to start/stop data acquisition.

Bandwidth

Use this property to specify the optical bandwidth at which a chromatogram is recorded.

Delta

Indicates the signal slope, that is, the difference between the current value and the value one second ago.

RefBandwidth

Use this property to average several photodiode signals of the reference signal. It is not necessary to select a reference bandwidth unless you enter a RefWavelength.

RefWavelength

Use this property to correct the absorption values of the wavelength that has been selected for the analysis. The selected reference wavelength should be in a quiet area of the spectrum where little absorption occurs.

Retention

Indicates the signal's retention time .

Signal

Indicates the current signal value [mAU] .

Wavelength

Use this property to set the wavelength for recording the signal on the UV channel to the wavelength with the absorbance maxima for the analytes of interest.

 

Equilibration commands and properties

Use the equilibration commands and properties only for the SmartStartup feature.

Command/Property

Description

Drift

Provides information about the detector Drift, determined by equilibration.

*.UpperLimit

Use this property to set the upper drift limit [mAU/h]. Set to 0 to turn drift equilibration off.

*.Value

Indicates the current drift value in mAU/h. The value is calculated as soon as at least a one-minute segment was measured. It is updated with each new recorded segment and averaged over the last 5 minutes.

DriftEquilibration

Indicates the status/result of the drift measurement.

DriftStatus

Indicates the status/result of the drift measurement.

 

N/A

Equilibration has not started.

 

Measuring

Equilibration is running, but the amount of data is not yet sufficient to report a result.

 

NotReady

Equilibration is running or has finished. The values are within the specified limits.

 

Good

Equilibration is running. The current data is outside the specified limits.

 

Failed

Equilibration is completed. The result is outside the specified limits.

 

NotTested

The limit was set to 0, drift measurement is disabled.

Equilibration

Provides information about the total status of the equilibration: OK or NotOK.

Noise

Provides information about the detector Noise.

*.UpperLimit

Use this property to set the upper noise limit in [mAU]. Set to 0 to turn noise equilibration off.

*.Value

Indicates the current noise. The value is calculated as soon as at least a one-minute segment was measured. It is updated with each new recorded segment and averaged over the last 5 minutes.

NoiseEquilibration

Indicates the status/result of the noise measurement: OK or NotOK.

NoiseStatus

Indicates the status/result of the noise measurement. For the available values, see DriftStatus.

StartEquilibration

Use this command start equilibration (noise/drift measurement).

 

General detector properties (read-only)

Command/Property

Description

Alarm

Indicates whether the detector reports an alarm. The detector will not clear an alarm automatically, manual intervention is required. Call MuteAlarm to mute the audible alarm.

AmbientTemp

Indicates the temperature [°C] outside the optical system.

ChannelIntensity1

Indicates an intensity value.

ChannelIntensity2

Indicates an intensity value.

ChannelIntensity3

Indicates an intensity value.

ChannelIntensity4

Indicates an intensity value.

ChannelIntensity5

Indicates an intensity value.

ChannelIntensity6

Indicates an intensity value.

ChannelIntensity7

Indicates an intensity value.

ChannelIntensity8

Indicates an intensity value.

ChannelIntensity9

Indicates an intensity value.

ChannelIntensity10

Indicates an intensity value.

DriverId

Indicates the unique driver identifier.

DriverManufacturer

Indicates the manufacturer of the driver.

DriverVersion

Indicates the version of the driver.

ExceptionLogClear

Use this command to clear the error log of the device.

 Note:

An error log is created if the firmware has crashed during an operation. The firmware sends all error log entries to the driver at connect time to be reported in the daily audit trail. You get a warning message about the error and are asked to send the affected audit trail to hardware service for inspection if this happens more often, and to use this command to clear the internal logs.

FirmwareVersion

Indicates the firmware version of the module.

FlowCellOperationTime

Indicates the time that the flow cell has been operated.

IlluminatedVolume_Flowcell

Indicates the illuminated volume of the flow cell.

LamphouseTemp

Indicates the lamp house temperature [°C].

LastUVLampChangeDate

Indicates when the UV lamp was replaced last.

Leak

Indicates whether the leak sensor has reported a leak.

LeftDoor

Indicates whether the compartment door is Open or Closed.

MaxPressure_Flowcell

Indicates the pressure limit of the flow cell.

ModelNo

Indicates the model number.

NotReadyCauses

Indicates why the module is not yet ready for the next analysis.

OperatingHours

Indicates the operating hours since the detector was operated for the first time.

OpticalPath_Flowcell

Indicates the optical path length of the flow cell.

PowerOnTime

Indicates the time since the detector was powered-up last.

PreviousUVLampOperation
Time

Indicates the operating hours of the previously installed UV lamp.

ProductNumber_Flowcell

Indicates the product number of the flow cell.

Qualification.LastDate

Indicates the date when detector qualification was performed last.

Qualification.LastOperator

Indicates the name of the person who performed the detector qualification.

Ready

Indicates that the module is ready for the next injection.

RightDoor

Indicates whether the compartment door is Open or Closed.

SerialNo

Indicates the serial number of the device.

SerialNo_Flowcell

Indicates the serial number of the flow cell.

SlitChangeCount

Indicates the number of times the slit has been changed.

SpectrographTemp

Indicates the temperature of the spectrograph.

Type_Flowcell

Indicates the flow cell type.

UvLamp_ProductNumber

Indicates the product number of the UV lamp.

UvLamp_SerialNo

Indicates the serial number of the UV lamp.

UVLampIgnitions

Counts the total number of successful UV lamp ignitions.

UVLampIntensity

Indicates the UV lamp intensity at 254 nm in counts per second.

UVLampOnTime

Counts the operating hours of the UV lamp since the lamp was ignited last.

UVLampOperationTime.Value

Indicates the total operating hours of the UV lamp.

WavelengthPeak1Measured

Indicates the measured peak of the first wavelength.

WavelengthPeak1Theoretical

Indicates the theoretical peak of the first wavelength.

WavelengthPeak2Measured

Indicates the measured peak of the second wavelength.

WavelengthPeak2Theoretical

Indicates the theoretical peak of the second wavelength.

WavelengthPeak3Measured

Indicates the measured peak of the third wavelength.

WavelengthPeak3Theoretical

Indicates the theoretical peak of the third wavelength.

WavelengthPeak4Measured

Indicates the measured peak of the fourth wavelength.

WavelengthPeak4Theoretical

Indicates the theoretical peak of the fourth wavelength.

WavelengthPeak5Measured

Indicates the measured peak of the fifth wavelength.

WavelengthPeak5Theoretical

Indicates the theoretical peak of the fifth wavelength.

WavelengthPeak6Measured

Indicates the measured peak of the sixth wavelength.

WavelengthPeak6Theoretical

Indicates the theoretical peak of the sixth wavelength.

WavelengthPeak7Measured

Indicates the measured peak of the seventh wavelength.

WavelengthPeak7Theoretical

Indicates the theoretical peak of the seventh wavelength.

 

General detector commands

Command

Description

AutoactivateUV_Lamp

Use this property to set the UV lamp. When set to On, the UV lamp is turned on automatically whenever the detector is powered up.

Autozero

Use this command to perform automatic null balancing (= the current detector signal is interpreted as 0).

BuzzerVolume

Use this property to specify the volume of the buzzer.

CalibrationReset

Use this command to reset all calibration settings to factory defaults.

Connect

Use this property to connect the device to the data system, enabling computer control.

Connected

Indicates whether the device is connected to the data system that is under computer control.

Data_Collection_Rate

Enter the rate [Hz] at which Chromeleon collects digital data from the detector.

DemoFileName

Use this property to enter the file name of the demo file (may contain %d, which will be replaced by the sample number).

Disconnect

Use this command to disconnect the device from the data system and enables manual control from the keypad of the device.

LampCover

Indicates whether the lamp cover is attached or not.

LeakSensorMode

Use this property to activate or deactivate leak detection.

  • Enabled (default and recommended): Activates leak detection. A beep alerts you when the leak sensor reports a leak.

  • Disabled: Deactivates leak detection. The leak sensor status is written to the Audit Trail, but no message appears and no beep sounds.

MuteAlarm

Use this property to mutes the audible alarm. The command has no effect if the alarm state is Off.

PeakWidth

Use this property to set the narrowest peak width at half height.

QualificationDone

Use this command when a qualification was done to update the associated information.

Parameter: At

desired wavelength

Parameter: doubleValue

double rounded as int (optional)

Parameter: index

Index (optional)

Parameter: intValue

intValue (optional)

Parameter: String

String

Parameter: strValue

strValue (optional)

Parameter: token

token (optional)

Parameter: Which

Defines which Thermo Scientific sensor has been added.

Reset

Use this command to reset the device to its initial condition, as attained after power-up.

ResponseTime

Use this property to specify the Response Time for the signal. The response time is the time required for the detector signal to rise from 10% to 90% in response to a signal increase. A longer response time reduces the noise. However, if the selected response time is too long, this can result in reduced peak heights and asymmetrical peak shapes.

The value calculated by Chromeleon is only a recommended value. You are free to select a different value as appropriate for your application.

 Tip:  

The response time multiplied by the data collection rate must not be smaller than 2 or greater than 20.

ServiceDone

Use this command when a service was done to update the associated information.

SetFactoryDefaults

Use this property to restore the Thermo Scientific standard settings.

Shutter

Use this property to specify whether the shutter blocks the light path.

SlitWidth

Use this property to specify the slit width. A wide slit allows more light to fall on the array. A smaller slit results in a higher optical resolution.

UV_Lamp

Use this property to indicate the state of the UV lamp. To turn on the deuterium lamp, set UV_Lamp to On.

 

UV calibration and validation commands

Command

Description

WavelengthCalibration

Use this command to perform wavelength calibration via the deuterium lamp.

 Note: 

To ensure that this command is executed correctly, a Wait UV.Ready command is required after this command in the PGM File.

WavelengthValidation

 

Use this command to perform an internal wavelength validation procedure using the holmium filter.

 Note: 

To ensure that this command is executed correctly, a Wait UV.Ready command is required after this command in the PGM File.

 

System Wellness and Predictive Performance commands and properties

 

Command/Property

Description

LastUVLampChangeDate

Indicates when the UV lamp was replaced last .

Qualification

Provides information about system qualification.

*.Interval

 

Use this property to specify the interval (in days) when the next system qualification is due.

*.WarningPeriod

Use this property to specify the period during which a warning appears before the next qualification is due.

*.GracePeriod

Use this property to specify the period during which the detector may be operated after the due date for re-qualification.

QualificationDone

Use this command after qualification to update the related system data.

Service

Provides detector service information.

*.LastDate

Indicates the date of the last service .

*.Interval

Use this property to specify the interval (in days) after which a service is due.

*.WarningPeriod

Use this property to specify the period during which a warning appears before the next service is due.

ServiceDone

Use this command after the device has been serviced, select this command to update the related system information.

SlitChangeCount

Indicates the number of times that the slit width has been changed.

UVLampOperationTime

Provides information on the UV lamp's operating time.

*.Limit

Use this property to set the limit for the operating time of the UV lamp. An error message appears when the specified value is reached.

*.Value

Indicates the total operating time of the UV lamp in [h].

*.Warning

Use this property to specify a time limit for issuing a warning with regard to the operation time. A warning appears when the specified value is reached.

 

Analog output commands and properties

The following commands and properties are available only if the DAC plug-in module is installed and the DAC Board check box is selected in the Properties dialog for the detector (Detector tab page) in the Server Configuration program.

Property

Description

Analog1_Offset
Analog2_Offset

Use this property to adjust the zero position of the analog output when it is plotted. The value entered is a percentage of the full-scale analog output. The offset allows the evaluation device to plot the signal if it becomes negative.

 Note: 

The output voltage of the analog outputs cannot reach a minimum of exactly 0 V. Therefore, we recommend to set an offset of at least 5 %, even if only positive analog output signals are expected. This will enable you to also measure very small output signals down to 0 precisely.

Analog1_Range
Analog2_Range

Use this property to set the voltage range of the analog output signal. The range to use depends on the evaluation device to which the output is connected.

Analog1_Resolution
Analog2_Resolution

Use this property to set the resolution of the analog output signal. The resolution to use depends on the value expected for the application.

 

Further Information

For an overview of the commands for all devices supported by Thermo Fisher Scientific, refer to Thermo Scientific: Commands and Tips.

For installation details, refer to Hardware Installation: Thermo Scientific Devices:

 Vanquish - Diode Array Detector.