Create Purification Samples/Fraction Analysis Samples Wizard:
Sample Properties

Determine the general properties for the purification or fraction samples (sample types: Preparation or Fraction):

 

Sample Properties:

Determine the properties for the samples to be created:

 

 

Program:

Enter the PGM File to be used for sample processing. To add a program, open the Browse dialog box and select a program.

 Tip:

If you have determined special conditions on the Conditional Program wizard page, the entry <Conditional Programs> appears in this field. In this case, the field cannot be edited.

 

 

Qnt. method:

Enter the QNT Method that shall be used for evaluating the samples. Follow the description for entering the PGM File (see above).

 

 

Type:

This field indicates the Sample Type of the samples to be created. The sample type is always Unknown. The entry cannot be edited.

 

 

Status:

This field indicates the Status of the samples to be created. The status is always Single. The entry cannot be edited.

 

 

In the list below, you may enter the values for the individual Sample Variables:

  • Click the {..} button or

  • Press ALT+PERIOD or

  • Press ALT+ENTER or

  • Double-click the respective line

To use a report variable, click the {..} button and select a variable in the Insert/Edit Sequence Title Label Variable dialog box.

 Note:

The default setting is usually {smp.x}. In this case, the value of the associated Analytic or Preparation variable is used.  
For all numerical floating point variables, such as Weight, ISTD Amount, and Dil. Factor, you may determine the number of positions after the decimal point. The default setting is ;4, e.g., {smp.amount;4}).

For the Name variable, the default setting for preparative samples is {smp.name} (prep), i.e., a space + (prep) is appended to the name of the original sample. The default settings for fraction samples is {smp.name} (fraction), i.e., a space + (fraction) is appended to the name of the original sample.

The default setting for the injection volume (Inj. Vol.) is 20.0µl.

 

For more information, refer to How to: Collecting Fractions Automatically (Autopurification)  Performing Autopurification.