Dionex Pumps
Dionex P680 HPLC Pump
In addition to the standard pump commands (see Dionex Pumps), the P680 pumps support the following commands and properties (please note that the display Filter level determines which commands and properties are displayed):
Command/Property |
Description |
AnalogOut |
Determines whether the pressure of the left or right pump is monitored via the Analog Out port on the pump (available for pumps with firmware 2.50.05 or higher). |
CamRevolutionsRight |
Indicates the number of revolutions of the camshaft of the right or left pump block. The CamRevolutionsLeft command is available for HPG pumps only. |
Curve |
Determines the curvature for flow gradients (see Gradient Curves). |
Degasser |
Turns the solvent rack degasser On or Off (P680A LPG-4, SOR-100, or SRD-3x00 only). The integrated degasser should always be on. |
DegasserVacuum |
Reports the status of the solvent rack degasser (P680A LPG-4, SOR-100, or SRD-3x00 only): OK or NotOK (read-only; available for pumps with firmware 2.03 or higher). |
HeadType |
Indicates the head type of the pump: Analytical or Semi-Prep (read-only). |
Leak |
Indicates the status of the central leak sensor: OK or Leak (read-only). |
LeakAlarm |
On indicates that there is a leak alarm (read-only; available for pumps with firmware 2.50.05 or higher). |
LeakAlarmOff |
Turns off the acoustic beep for the current alarm (available for pumps with firmware 2.50.05 or higher). |
LeakDelay |
Specifies how much time elapses between the detection of a leak and the pump shutdown (available for pumps with firmware 2.50.05 or higher). |
LeakSensorMode |
Specifies how leak detection is performed: |
MaximumFlowRamp |
Specifies the upper limit for the flow rate acceleration |
ModelVariant |
Indicates the variant: Isocratic, LPG, or HPG (read-only). |
Motor |
Indicates whether the pump is delivering: On or Off (read-only). |
Pump_Pressure |
Commands and properties for the pressure signal (see below). |
Enables purging when set to On (available for pumps with firmware 2.50.06 or higher). |
|
PurgeFlow |
Enter the flow [in mL/min] to be delivered by the pump during purging (range: 0.000 to 10.000 ml/min or 20.000 ml/min for HPG pumps with enabled Double Flow option; available for pumps with firmware 2.50.05 or higher). |
PurgeTime |
Specifies for how long purging is performed (0 - 1000 s) (available for pumps with firmware 2.50.05 or higher). |
RearSealLeakCounter |
Indicates the number of drops that passed the piston seal in the past hour. |
RearSealLeakLimit |
Specifies the leak detection threshold for the rear seal wash system. If the limit is met, a message is displayed in the Audit Trail and on the pump. |
RearSealWashPump |
Indicates whether the peristaltic pump of the rear seal wash system is running (Active) or not (Idle) (read-only). |
RearSealWashSystem |
Turns the rear seal wash system on (Interval or Automatic) or Off. Interval-Activates rear-seal washing for 5 minutes every hour. However, the drop sensor on the liquid reservoir is not active, i.e., the piston seals are not monitored for tightness. Automatic-Periodically activates rear-seal washing once per hour until the drop sensor has counted 50 drops. The drop sensor is active, i.e., the piston seals are monitored for tightness. Off-Turns the rear-seal wash system off. |
SelfTest |
Performs a self-test to check that all main components are functioning correctly. |
SelfTestPassed |
Reports the results of the self-test (read-only). If the pump fails the test, eliminate the cause of the error and/or fault. For troubleshooting help, refer to the operator's manual for the pump. |
SolventRackLeak |
Reports whether the leak sensor in the solvent rack detected a leak: Leak or NoLeak (read-only; available for pumps with firmware 2.03 or higher). |
WorkLoadLeft |
Indicates the workload of the left pump block in [MJ] (read-only). The WorkLoadLeft command is available for HPG pumps only. |
WorkLoadRight |
Indicates the workload of the right pump block in [MJ] (read-only). |
Pump_Pressure
If you select the Pressure Signal(s) check box on the Devices page in the Server Configuration program, Chromeleon records the pump pressure as a separate channel (Pump_Pressure). The following commands and properties are available:
AcqOn starts data acquisition. AcqOff terminates data acquisition. |
|
Averages all measured values. |
|
Reports the signal's slope, i.e., the difference between the value and the value 1 second ago (read-only). This is useful for Triggers. |
|
Sets the maximum step rate for Step = Auto. |
|
Retention |
Indicates the retention time for the signal. |
Sets the step for data acquisition. |
Equilibration Commands and Properties
Tip:
Use the equilibration commands and properties only for the SmartStartup feature.
Equilibration |
Reports the equilibration status. |
|
Ripple |
Reports the ripple of the pump pressure. |
|
UpperLimit |
Determines the upper limit for the ripple of the pressure signal in [%]. The upper limit can be any value between 1.0% and 5.0%. The default setting is 3.0%. |
|
Value |
Reports the actual value. The value is calculated as soon as at least a one-minute segment was measured. It is updated with each new recorded segment and averaged over the last 5 minutes. If the average pressure is below 10 bar, the ripple measurement is started again. The value of the property does not change after the measurement and is displayed under Preconditions. |
|
RippleStatus |
Reports the ripple equilibration status of the pump pressure (read-only). |
|
N/A |
Equilibration has not started. |
|
Measuring |
Equilibration is running, but the amount of data is not yet sufficient to report a result. |
|
Good |
Equilibration is running or has finished. The values are within the specified limits. |
|
NotReady |
Equilibration is running. The current data is outside the specified limits. |
|
Failed |
Equilibration is completed. The result is outside the specified limits. |
|
NotTested |
The limit was set to 0, thus disabling ripple checking. |
|
StartEquilibration |
Starts equilibration. For more information, refer to How to ...: Equilibrating the Chromatography System. |
For information about how to install the pump, refer to Hardware Installation P680 HPLC Pump: Overview in the Administrator Help section.