Dionex Detectors
Dionex UltiMate 3000 Series (RS)/ICS-Series Variable Wavelength Detectors

In addition to the standard commands available for all detectors (see  Dionex Detectors), the VWD-3x00 and ICS-Series VWD detectors provide the control commands listed below. Please note that the display Filter level determines which commands and properties are displayed. Also note that some commands or properties may not be available, depending on the detector type.

 

Command/Property

Description

AmbientTemp

Reports the temperature [°C] outside the optical system (read-only).

AutoactivateUV_Lamp

On: The UV lamp is turned on automatically whenever the detector is powered up.

AutoactivateVisible_Lamp

On: The visible lamp is turned on automatically whenever the detector is powered up.

Autozero

Performs automatic null balancing (= the current detector signal is interpreted as 0).

BaselineBehavior

Determines how the baseline behaves if wavelengths are switched or the sensitivity or filter wheel setting are changed during a program:

Append: Resets the baseline to the previous signal.

Free: No adjustment, shifts may occur in the baseline position.

Zero: Sets the baseline to zero.

BootLoaderVersion

Reports the bootloader version (read-only).

Brightness

Adapts the brightness of the detector's front panel display to your requirements.

ClearAlarmLED

Resets the Status LED on the detector's front panel when it indicates an alarm.

ClearBaseline

Deletes the most recent baseline scan from the memory. (Also, see Scan and ScanBaseline).

ClearDisplayError

Deletes the error messages on the detector's display.

Contrast

Adapts the screen contrast of the detector's front panel display to your requirements.

Data_Collection_Rate

Enter the rate [Hz] at which Chromeleon collects digital data from the detector

DeviceType

Indicates the detectors device type (read-only).

DisplayMode

Specifies which type of data appears on the detector's front panel display (Raw, Transmittance, or Absorbance).

Door

Reports whether the compartment door is Open or Closed (read-only).

DriverID

Indicates the driver's unique name (read-only).

DriverVersion

Indicates the driver version (read-only).

ElectronicsTemp

Indicates the temperature [°C] of the electronics unit (read-only).

FlowcellType

Indicates the flow cell type (read-only).

FPGAVersion

Indicates the detector's FPGA version (read-only).

HardwareRevision

Indicates the detector's hardware revision (read-only).

HardwareRevision_
Optics

Indicates the optics' hardware revision (read-only).

LamphouseTemp

Indicates the lamp house temperature [°C] (read-only).

Leak

Indicates whether the leak sensor has detected a leak: NoLeak or Leak (read-only).

LeakDelay

Reports the delay time [s] after a leak was detected

LeakSensorMode

Specifies how leak detection is performed:
Enabled - Enables leak detection; an acoustic beep sounds when the leak sensor is activated.
Silent - Enables leak detection, but no beep sounds when the leak sensor is activated.
Disabled - Disables leak detection.

Manufacturer

Indicates the manufacturer of the driver (read-only).

NotReadyCauses

Reports why the module is not yet ready for the next analysis (read-only).

OpticsTemp

Reports the temperature [°C] of the optics (read-only).

Ready

Indicates whether the detector is ready for injection (read-only).

Reset

Resets the device to its initial conditions, as attained after power-up.

Scan

Saves an absorbance spectrum based on the current settings to a spectra library. This requires that a baseline spectrum was recorded with exactly identical parameters (see ScanBaseline). For information about how to perform a wavelength scan, refer to Detector Control  Wavelength Scanning.

ScanBaseline

Saves a baseline scan based on the current settings to a spectra library. (Also, see ClearBaseline and Scan.)

ScanEndWavelength

Sets the end wavelength  [nm] of the wavelength range for spectra scan. The allowed range is 190 to 900 nm. (Also, see ScanBaseline and Scan.)

ScanSpeed

Defines the speed with which a wavelength range (defined by start and end wavlength) is scanned. (Also, see ScanBaseline and Scan.)

ScanStartWavelength

Sets the start wavelength [nm] of the wavelength range for spectra scan. The allowed range is 190 to 900 nm. (Also, see ScanBaseline and Scan.)

SerialNo_Flowcell

Reports the serial number of flow cell (read-only).

SerialNo_Mainboard

Reports the serial number of the main board (read-only).

SerialNo_Optics

Reports the serial number of the optics (read-only).

SetFactoryDefaults

Restores the Dionex standard settings.

Standby

Switches the detector to standby mode (Standby) or cancels standby mode (NoStandby). During standby mode, the detector remains connected in Chromeleon. Available values: Standby, NoStandby, WakingUp, EnteringStandby. (WakingUp and EnteringStandby are temporary states that the device assumes automatically; it is therefore neither required nor reasonable to select these values from the commands list.)

StopScan

Stops a running scan of a baseline or absorbance spectrum. (Also, see ScanBaseline and Scan.)

TimeConstant

Specify the time constant for the signal. The time constant is the time required for the detector signal to rise from 0% to 63% in response to a signal increase. The constant is used for noise suppression (values: 0.00 to 4.55 s; depending on the detector type only a predefined scale of values may be available). The time constant is directly associated with the Rise_Time. The following formula applies: 2.2 x TimeConstant = Rise Time.

The value calculated by Chromeleon is a recommendation only. A different value can be selected, if appropriate for your application.

 Tip:  

Most noise is suppressed if the time constant is 4.55 s. However, for the acquisition of narrow peaks, a lower time constant is more appropriate.

UV_Lamp

Reports the state of the UV lamp: Error, Ignition, Off, On.

UvLamp_ProductNumber

Indicates the product number of the UV lamp (read-only).

UvLamp_SerialNo

Indicates the serial number of the UV lamp (read-only).

UvTransmission_Flowcell

Indicates the factor for calculation of absorption to take the typical transmission for the flow cell into account (read-only). If the flow cell has a chip, the values are read from the chip. Otherwise, the value 100 is used.

Visible_Lamp

Reports the visible lamp's state: Error, Ignition, Off, On.

VisLamp_ProductNumber

Indicates the product number of the visible lamp (read-only).

VisLamp_SerialNo

Indicates the serial number of the visible lamp (read-only).

VisTransmission_Flowcell

Indicates the factor for calculation of absorption to take the typical transmission for the flow cell into account (read-only). If the flow cell has a chip, the values are read from the chip. Otherwise, the value 100 is used.

WavelengthCalibration

Performs wavelength calibration. In addition, wavelength calibration is performed automatically whenever the detector is powered up. (Also, see WvlCalibStatus)

WavelengthPeak1/2/3
Measured

Reports the measured wavelength for peaks 1, 2, or 3.

WavelengthPeak1/2/3
ResultMeasm

Reports the result (pass or fail) of the wavelength measurement for peaks 1, 2, or 3.

WavelengthPeak1/2/3
Theoretical

Reports the wavelengths expected for peaks 1, 2, or 3 when the wavelength verification test is performed via the Holmium Oxide Filter.

WavelengthVerTest

Performs wavelength verification via the holmium oxide filter. For detailed information also refer to the operating instructions of the detector.

WavelengthVerTest
Result

Reports the result (pass or fail) of the wavelength verification. (Also, see WavelengthVerTest.) The test results are also recorded in the Audit Trail.

WvlCalibStatus

Indicates the status of the wavelength calibration (read-only): Initialized, Running, Calibrated, Error (Also, see WavelengthCalibration)

 

Analog Output commands

  Note:

The commands for configuring the analog outputs are available only if the detector is fitted with a DAC plug-in module and if the DAC Board check box is selected on the Detector page in the Properties dialog for the detector.

 

Command/Property

Description

Analog1_Mode
Analog2_Mode

Sets the signal that is available at analog output. Depending on the channel of interest, select  
Abs_A
(B, C, or D) for the absorption or
Measm_A
(B, C, or D) for the measurement channel  or
Ref_A
(B, C, or D) for the reference channel
(The setting Direct is reserved for Dionex Service and should not be selected.)

Analog1_Offset
Analog2_Offset

Adjusts the zero position of the analog output when it is plotted. The value entered is a percentage of the full-scale analog output. The offset allows the evaluation device to plot the signal if it becomes negative.

 Note: 

The output voltage of the analog outputs cannot reach a minimum of exactly 0 V. Therefore, we recommend to set an offset of at least 5 %, even if only positive analog output signals are expected. This will enable you to also measure very small output signals down to 0 precisely.

Analog1_Range
Analog2_Range

Sets the voltage range, and thus the resolution of the analog output signal. The range to use depends on the values expected for the application and the evaluation devices to which the output is connected.  Available values are:

1AU_per_1V=0, 01AU_per_1V=1, 5AU_per_1V=2, 1AU_per_10V=3, 01AU_per_10V=4, 5AU_per_10V=5

 

UV_VIS channel commands

 

Command/Property

Description

MaxAutoStep

Sets the maximum step for the Auto-Step mode. (The available range is from 0.1 to 5.1 s, the default is 5.1 s.)

Retention

Reports the signal's retention time (read-only).

Signal

Reports the current signal value [mAU] (read-only).

Step

Sets the step.

Wavelength

Sets the wavelength.  (The available range is from 190 to 900 nm.)

 

Equilibration commands and properties

Use the equilibration commands and properties only for the SmartStartup feature.

Command/Property

Description

Drift

Provides information about the detector Drift, determined by equilibration.

*.UpperLimit

Sets the upper drift limit [mAU/h]. Available values are: 0.8 and 20.0 mAU/h.

*.Value

Reports the current drift value in mAU/h. The value is calculated as soon as at least a one-minute segment was measured. It is updated with each new recorded segment and averaged over the last 5 minutes. The property value does not change after measurement and can be viewed in the Precondition Log (Preconditions) of the subsequent samples.

DriftEquilibration

Reports the status/result of the drift measurement: OK or NotOK (read-only).

DriftStatus

Reports the status/result of the drift measurement (read-only).

 

N/A

Equilibration has not started.

 

Measuring

Equilibration is running, but the amount of data is not yet sufficient to report a result.

 

NotReady

Equilibration is running or has finished. The values are within the specified limits.

 

Good

Equilibration is running. The current data is outside the specified limits.

 

Failed

Equilibration is completed. The result is outside the specified limits.

 

NotTested

The limit was set to 0, drift measurement is disabled.

Equilibration

Provides information about the total status of the equilibration: OK or NotOK (read-only).

Noise

Provides information on the detector Noise.

*.UpperLimit

Sets the upper noise limit in [mAU]. The allowed range is: 0.03 to 0.50 mAU.

*.Value

Indicates the current detector noise. Usually, this is the value averaged over 5 minutes (read-only). Also, see Drift.Value.

NoiseEquilibration

Reports the status/result of the noise measurement: OK or NotOK (read-only).

NoiseStatus

Reports the status/result of the noise measurement (read-only). For the available values, see DriftStatus.

StartEquilibration

Starts equilibration (noise/drift measurement).

 

System Wellness and Predictive Performance commands and properties

 Tip:  

The Chromeleon version and detector type determine which commands and properties are available for checking the detector's system wellness and performance.

 

Command/Property

Description

FilterMovements

Counts the movements of the holmium oxide filter (read-only).

GratingMovements

Counts the movements of the grating (read-only).

LastUVLampChangeDate

Reports when the UV lamp was replaced last (read-only).

LastVISLampChangeDate

Reports when the visible lamp was replaced last (read-only).

OperatingHours

Counts the operating hours since initial operation (excluding the operating hours in standby mode (read-only).

PowerOnTime

Counts the time since last power-up (or last wake-up from standby) (read-only).

PreviousUVLampOperation
Time

Reports the operating hours of the previously installed UV lamp (read-only).

PreviousVISLampOperation
Time

Reports the operating hours of the previously installed visible lamp (read-only).

Qualification

Provides information about system qualification.

*.LastDate

Reports the date when detector qualification was performed last (read-only).

*.LastOperator

Reports the name of the person who performed the detector qualification (read-only).

*.Interval

 

Reports the interval (in days) when the next system qualification is due.

*.WarningPeriod

Specifies the period during which a warning appears before the next qualification is due.

*.GracePeriod

Indicates the period during which the device may be operated after the due date for re-qualification.

QualificationDone

Perform this command after qualification to update the related system data.

Service

Provides detector service information.

*.LastDate

Reports the date of the last service (read-only).

*.Interval

Specify the interval (in days) after which a service is due.

*.WarningPeriod

Specifies the period during which a warning appears before the next service is due.

ServiceDone

After the device has been serviced, perform this command to update the related information.

StandbyHours

Counts the total operating hours in standby mode since the module was operated for the first time (read-only).

UpdateLampIntensity

Updates the lamp intensity values.

UVLampIgnitions

Counts the total number of successful UV lamp ignitions (read-only).

UVLampIgnitionCurrent
Trials

Reports the number of ignition trials when the UV lamp was started last (read-only).

UVLampIgnitionFailures

Counts how many times the UV lamp ignition fails (read-only). After a maximum of 10 retries, the counter is incremented by one.

UVLampOnTime

Counts the operating hours of the UV lamp since the lamp was ignited last (read-only).

UVLampOperationTime

Provides information on the UV lamp's operating time.

*.Value

Reports the total operating hours of the UV lamp (read-only).

*.Warning

A warning appears when the specified value is reached.

*.Limit

An error message appears when the specified value is reached.

UVRelIntensity

Provides information regarding the relative intensity of the UV lamp.

*.Value

Reports the current relative intensity of the UV lamp (read-only). The intensity of the UV lamp is measured at 230 nm, independent of the measuring wavelength set with the Wavelength command. 100% corresponds to the value that was measured and stored on the reference channel after 100 lamp operating hours.

*.Warning

A warning appears when the specified value is reached.

*.Limit

An error message appears when the specified value is reached.

VISLampIgnitionFailures

Counts how many times the visible lamp ignition fails (read-only). After a maximum of 10 retries, the counter is incremented by one.

VISLampIgnitions

Counts the total number of successful visible lamp ignitions (read-only).

VISLampOnTime

Counts the operating hours of the visible lamp since the lamp was ignited last (read-only).

VISLampOperationTime

Provides information on the visible lamp's operating time.

*.Value

Reports the total operating hours of the visible lamp (read-only).

*.Warning

A warning appears when the specified value is reached.

*.Limit

An error message appears when the specified value is reached.

VISRelIntensity

Provides information regarding the relative intensity of the visible lamp.

*.Value

Reports the current relative intensity of the visible lamp (read-only). The intensity of the Vis lamp is measured at 700 nm, independent of the measuring wavelength set with the Wavelength command. 100% corresponds to the value that was measured and stored on the reference channel after 100 lamp operating hours.

*.Warning

A warning appears when the specified value is reached.

*.Limit

An error message appears when the specified value is reached.

 

For practical tips for control commands in programs, refer to   Tips for Creating Programs (VWD-3x00).

For PCM-3000 pH and conductivity monitor commands and properties, refer to UltiMate 3000 Series VWD, DAD and MWD Detectors: pH and Conductivity Monitor Commands.

For information about how to install the detector, refer to:

Hardware Installation  UltiMate 3000 Series - Variable Wavelength Detector: Overview

 ICS-Series Variable Wavelength Detector: Overview