Temperature Control
Controlling the Sample Temperature

Some autosamplers (for example, Dionex ASI-100T and WPS-3000T), have a thermostatting option that allows you to cool the samples.

You can then control the temperature of the instrument by using the corresponding control (gauge or edit field) on the Control Panel.

To change the temperature during operation

As a rule, a Panel Tabset or Control Panel for an autosampler with thermostatting option provides control elements for reporting the current temperature, as well as for setting a new nominal temperature. If this is not the case for your autosampler, you can add such a control element to a panel (see  Modifying a Control Panel).

To control the temperature using a program

Use the Program Wizard to create a program as described in  Automatically Creating a Program. One of the wizard pages refers to autosampler sample thermostatting. On this page, verify that the check box for enabling temperature control is selected and enter the desired values in the fields below.

Program Example (here: WPS-3000T)

 

0.000

Sampler.TempCtrl

= On

;

This command enables and disables the temperature control.

 

0.000

Sampler.Temperature.Nominal

= Value[°C]

;

This command sets the nominal temperature.

0.000

Sampler.Temperature.UpperLimit

= Value[°C]

0.000

Sampler.Temperature.LowerLimit

= Value[°C]

;

;

These commands define the upper and lower limit.

The limits are monitored by Chromeleon.

0.000

Wait

Temperature.Ready

;
;
;

;

The Wait command delays all further operations on

the instrument until the system receives the feedback

that the nominal temperature has been reached.